TY - JOUR KW - Atomic force microscopy KW - Polarization KW - Epitaxial growth KW - Scanning tunneling microscopy (STM) KW - Ferroelectric thin films KW - Relative orientation KW - Domain structure KW - SrTiO KW - Piezoresponse KW - In-plane polarization KW - Out-of-plane KW - Polydomain KW - Atomic force microscope (AFM) KW - Differential signal KW - Polarization vectors AU - C.S Ganpule AU - V Nagarajan AU - B.K Hill AU - A.L Roytburd AU - E.D Williams AU - Ramamoorthy Ramesh AU - S.P Alpay AU - A Roelofs AU - R Waser AU - L.M Eng AB - Voltage-modulated scanning force microscopy (Piezoresponse microscopy) is applied to investigate the domain structure in epitaxial PbZr 0.2Ti 0.8O 3 ferroelectric thin films grown on (001) SrTiO 3. By monitoring the vertical and lateral differential signals from the photodetector of the atomic force microscope it is possible to separate out and observe the out-of-plane and in-plane polarization vectors in the thin film individually. The relative orientation of the polarization vectors across a 90° domain wall is observed. Nucleation of new reversed 180° domains at the 90° domain wall is studied and its impact on the rotation of polarization within the a domain is analyzed as a function of reversal time. © 2002 American Institute of Physics. BT - Journal of Applied Physics DO - 10.1063/1.1421219 LA - eng M1 - 3 N1 - cited By 121 N2 - Voltage-modulated scanning force microscopy (Piezoresponse microscopy) is applied to investigate the domain structure in epitaxial PbZr 0.2Ti 0.8O 3 ferroelectric thin films grown on (001) SrTiO 3. By monitoring the vertical and lateral differential signals from the photodetector of the atomic force microscope it is possible to separate out and observe the out-of-plane and in-plane polarization vectors in the thin film individually. The relative orientation of the polarization vectors across a 90° domain wall is observed. Nucleation of new reversed 180° domains at the 90° domain wall is studied and its impact on the rotation of polarization within the a domain is analyzed as a function of reversal time. © 2002 American Institute of Physics. PY - 2002 SP - 1477 EP - 1481 T2 - Journal of Applied Physics TI - Imaging three-dimensional polarization in epitaxial polydomain ferroelectric thin films VL - 91 SN - 00218979 ER -